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#test-results 2024-06-02

Sunday23 messages6 participantstimes are UTC
Highlights from this day
  • LC_MS_Lena — a result without a lot number and a purchase date is an anecdote with a pdf attached 23:04
  • lot_number_lou — i told QST about a result they would not have liked and they did not argue. credit where it is due 23:16
  • HPLC_Hank — my read after three years of this: purity is mostly fine across the market and fill consistency is where suppliers differ one bad test does not condemn a supplier.… 23:18
  • private_script_pri — the widest spread in my data is about 2.6 percentage points across five lots from one supplier 23:33
  • split_dose_sam — post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later 23:40
LM

a result without a lot number and a purchase date is an anecdote with a pdf attached

💀16🧊4

weigh it first

LM

posting my PeptideMeter result on lot C-4402, what do people make of it

weigh the vial before you reconstitute. it costs nothing and catches the common failure

LM

ok so sample handling on your end absolutely affects it. draw cleanly, ship fast, do not let it sit warm

[edited]
LN

i told QST about a result they would not have liked and they did not argue. credit where it is due

HH

my read after three years of this: purity is mostly fine across the market and fill consistency is where suppliers differ
one bad test does not condemn a supplier. one good test does not clear one. both halves get ignored equally

while im here update from 24 months ago: retested the same supplier, result came back better, logged both

PS

what interests me is when the gap goes the same direction every time. once is noise, three times is a pattern

*VendorInvestigate not the other one

quick one how much does sample handling on my end affect the number

PS

the widest spread in my data is about 2.6 percentage points across five lots from one supplier

📈16⚠️3❤️8

a supplier disputing a result is rare here and it has never gone well for the supplier

post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later

SD

quick one a single sample tells you about a single vial. that is genuinely all it tells you

AP

certificate said 98.6 and the independent came back 97.4, is that a problem

AP

my vial assayed under label but the purity was fine, which matters more