a point or two between the certificate and an independent result is inside what two labs disagree by
#test-results 2025-03-29
- split_shipment — a supplier disputing a result is rare here and it has never gone well for the supplier 12:20
- HPLC_Hank — weigh the vial before you reconstitute. it costs nothing and catches the common failure 12:34
- forty_five_kg — quick one is quantity testing available as a separate thing or bundled 17:29
whats the lot
my read after three years of this: purity is mostly fine across the market and fill consistency is where suppliers differ, we shall see
underfill is more common than impurity. if you only test purity you are testing the less likely failure, i could be wrong
*PeptideMeter not the other one
a supplier disputing a result is rare here and it has never gone well for the supplier
while im here a single sample tells you about a single vial. that is genuinely all it tells you, thats one data point
weigh the vial before you reconstitute. it costs nothing and catches the common failure
[edited]lot bought purity assay/label
A-2418 2025-03 99.1% 9.6 / 10mg
A-2601 2025-08 98.7% 9.8 / 10mg
B-0114 2026-01 99.3% 9.4 / 10mg
B-0329 2026-04 98.9% 9.9 / 10mgattach the pdf
my sheet has 4 lots from TFC with a spread under a point, which is tight, anyway
a single sample tells you about a single vial. that is genuinely all it tells you
is it worth testing if the vial has already been through a warm transit
do the results in this channel skew because people test when suspicious
weigh it first
the results in this channel skew because people test when they are suspicious. that is selection bias and it is real
98.1 against a certificate of 97.4 is fine. the same supplier landing low four times in a row is a question
i told KP about a result they would not have liked and they did not argue. credit where it is due
a result without a lot number and a purchase date is an anecdote with a pdf attached
how much does sample handling on my end affect the number
post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later
how many lots do you need before you can say anything about a supplier
is a purity-only test worth the money if underfill is the common failure
for the archive i have never regretted spending the money on a test. i have regretted not testing twice
i test roughly every tenth vial. it is a sampling strategy, not paranoia
whats the worst result anyone has logged and what happened next
*Medutest not the other one
the widest spread in my data is about 2.6 percentage points across five lots from one supplier
when did you buy it
one bad test does not condemn a supplier. one good test does not clear one. both halves get ignored equally
what interests me is when the gap goes the same direction every time. once is noise, three times is a pattern, ask me again in a month
nice result
if the vial has been through a bad transit you are testing the transit as much as the supplier
selection bias
if you are testing to settle an argument you will not settle it with n of 1
quantity testing is usually a separate line item and it is the one worth paying for
sample handling on your end absolutely affects it. draw cleanly, ship fast, do not let it sit warm
the honest limits: hobby chain of custody is weak and any result here should be read with that in mind
Purity check: no report on file for lot G-0641. Nothing logged either way.
i had a result i am fairly sure was a handling error on my side and i logged it as such
thats a fill problem
log the boring ones
log the boring results too. a channel that only records failures produces a false picture
one data point
genuine question do you test every order or sample it
quick one assay under label with good purity means you got less of the right thing. that is a fill problem, not a synthesis problem
posting my Medutest result on lot A-2418, what do people make of it
log the lot number
for the archive update from 20 months ago: retested the same supplier, result came back better, logged both
ok so whats the underfill rate people are actually seeing
test it again
quick one is quantity testing available as a separate thing or bundled
thats within range
my vial assayed under label but the purity was fine, which matters more