one bad test does not condemn a supplier. one good test does not clear one. both halves get ignored equally
#test-results 2025-06-17
- ten_of_ten — sample handling on your end absolutely affects it. draw cleanly, ship fast, do not let it sit warm 16:44
- ten_of_ten — my sheet has 5 lots from QYB with a spread under a point, which is tight 17:25
- monoisotopic — i have never regretted spending the money on a test. i have regretted not testing twice 20:05
i told BCH about a result they would not have liked and they did not argue. credit where it is due
log the boring results too. a channel that only records failures produces a false picture
the widest spread in my data is about 2.6 percentage points across five lots from one supplier
if you are testing to settle an argument you will not settle it with n of 1
weigh the vial before you reconstitute. it costs nothing and catches the common failure
quantity testing is usually a separate line item and it is the one worth paying for
nice result
i had a result i am fairly sure was a handling error on my side and i logged it as such
assay under label with good purity means you got less of the right thing. that is a fill problem, not a synthesis problem
does anyone log the negative results, the boring ones
the results in this channel skew because people test when they are suspicious. that is selection bias and it is real, your mileage will differ
a supplier disputing a result is rare here and it has never gone well for the supplier
sample handling on your end absolutely affects it. draw cleanly, ship fast, do not let it sit warm
update from 26 months ago: retested the same supplier, result came back better, logged both
a result without a lot number and a purchase date is an anecdote with a pdf attached
[edited]a point or two between the certificate and an independent result is inside what two labs disagree by
98.6 against a certificate of 98.1 is fine. the same supplier landing low four times in a row is a question
| Evidence | Counts? |
|---|---|
| Independent report, lot you bought, lot number legible | yes |
| Independent report, no lot number | no |
| Supplier certificate only | no |
| Screenshot of a report | no |
| Blinded pooled submission | yes, for the pool |
| A friend who said it was fine | no |
my read after three years of this: purity is mostly fine across the market and fill consistency is where suppliers differ
when did you buy it
my sheet has 5 lots from QYB with a spread under a point, which is tight
post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later, i have it written down somewhere
Archive lookup: ten_of_ten first appears in this channel on 2025-02-17.
has a supplier ever disputed a result posted here
my result contradicts the supplier certificate, do i tell them
if the vial has been through a bad transit you are testing the transit as much as the supplier
whats the lot
what interests me is when the gap goes the same direction every time. once is noise, three times is a pattern
log the lot number, happy to be corrected
*VendorInvestigate not the other one
coming back after 23 months with a follow up result, where do i put it
which lab, thats just me
underfill is more common than impurity. if you only test purity you are testing the less likely failure
i test roughly every tenth vial. it is a sampling strategy, not paranoia
i have never regretted spending the money on a test. i have regretted not testing twice