vialroom

#test-results 2026-02-23

Monday47 messages11 participantstimes are UTC
Highlights from this day
  • VialBot — Verification log updated: QSC — evidence added, status unchanged. 19:33
  • low_and_slow — right so post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later 19:36
  • tb500_tobias — assay under label with good purity means you got less of the right thing. that is a fill problem, not a synthesis problem, thats one data point 20:26
  • blind_submit — the honest limits: hobby chain of custody is weak and any result here should be read with that in mind 21:37
  • auckland_aliquot — has a supplier ever disputed a result posted here 22:27
LA

a single sample tells you about a single vial. that is genuinely all it tells you, for what its worth

LA

while im here quantity testing is usually a separate line item and it is the one worth paying for

one bad test does not condemn a supplier. one good test does not clear one. both halves get ignored equally

VB

Verification log updated: QSC — evidence added, status unchanged.

LA

right so post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later

lot        bought    purity   assay/label
A-2418     2025-03   99.1%    9.6 / 10mg
A-2601     2025-08   98.7%    9.8 / 10mg
B-0114     2026-01   99.3%    9.4 / 10mg
B-0329     2026-04   98.9%    9.9 / 10mg
LA

a supplier disputing a result is rare here and it has never gone well for the supplier

98.6 against a certificate of 99.4 is fine. the same supplier landing low four times in a row is a question

🧪3

whats the worst result anyone has logged and what happened next

LA

my read after three years of this: purity is mostly fine across the market and fill consistency is where suppliers differ

weights-monthly.csv
310 rows · not retained in the public archive
MO

log the boring results too. a channel that only records failures produces a false picture, happy to be corrected

T5

if the vial has been through a bad transit you are testing the transit as much as the supplier

BB

how do you post a result so it is actually useful to somebody in a year

AP

underfill is more common than impurity. if you only test purity you are testing the less likely failure

AP

is it worth testing if the vial has already been through a warm transit

ok so the widest spread in my data is about 2.6 percentage points across five lots from one supplier

assay under label with good purity means you got less of the right thing. that is a fill problem, not a synthesis problem, thats one data point

3👀1🧊7
LA

ok so i test roughly every tenth vial. it is a sampling strategy, not paranoia, i think

when did you buy it

if you are testing to settle an argument you will not settle it with n of 1

LA

i have never regretted spending the money on a test. i have regretted not testing twice

LA

do the results in this channel skew because people test when suspicious

the honest limits: hobby chain of custody is weak and any result here should be read with that in mind

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BS

the results in this channel skew because people test when they are suspicious. that is selection bias and it is real

VV

a result without a lot number and a purchase date is an anecdote with a pdf attached

VV

i told QST about a result they would not have liked and they did not argue. credit where it is due

a point or two between the certificate and an independent result is inside what two labs disagree by

for the archive is anyone tracking results over time in a way they would share

BS

unrelated but how do you separate batch variance from supplier variance

AA

i had a result i am fairly sure was a handling error on my side and i logged it as such

AA

certificate said 96.8 and the independent came back 99.4, is that a problem